Method of synthesis and structure of (5E)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1H-pyrrole-3-carboxylates / Mukovoz P.P., Koz'minykh V.O., Andreeva V.A., El'tsov O.S., Slepukhin P.A., Koz'minykh E.N. // Russian Journal of Organic Chemistry. - 2015. - V. 51, l. 6. - P. 860-863.

ISSN:
10704280
Type:
Article
Abstract:
Abstract A procedure has been developed for the synthesis of dialkyl (5E)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1H-pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and p-toluidine. The structure of the products is discussed on the basis of the IR, 1H NMR, and X-ray diffraction data. © 2015 Pleiades Publishing, Ltd.
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DOI:
10.1134/S107042801506007X
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https://www.scopus.com/inward/record.uri?eid=2-s2.0-84938091025&doi=10.1134%2fS107042801506007X&partnerID=40&md5=5455617f1963c112769fbd293ad65b7e
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Art. No. 1062
Link https://www.scopus.com/inward/record.uri?eid=2-s2.0-84938091025&doi=10.1134%2fS107042801506007X&partnerID=40&md5=5455617f1963c112769fbd293ad65b7e
Affiliations Institute for Cellular and Intracellular Symbiosis, Ural Branch, Russian Academy of Sciences, ul. Pionerskaya 11, Orenburg, Russian Federation; Perm State Humanitarian-Pedagogical University, Sibirskaya ul. 24, Perm, Russian Federation; Orenburg State University, pr. Pobedy 13, Orenburg, Russian Federation; Yeltsin Ural Federal University, ul. Mira 19, Yekaterinburg, Russian Federation; Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, ul. S. Kovalevskoi/Akademicheskaya 22/20, Yekaterinburg, Russian Federation
References Perevalov, S.G., Burgart, Ya.V., Saloutin, V.I., Chupakhin, O.N., (2001) Russ. Chem. Rev., 70 (11), p. 921; Koz'Minykh, V.O., Igidov, N.M., Zykova, S.S., Kolla, V.E., Shuklina, N.S., Odegova, T.F., (2002) Pharm. Chem. J., 36 (4), p. 188; Yamashkin, S.A., Zhukova, N.V., (2008) Chem. Heterocycl. Compd., 44 (2), p. 115; Zykova, S.S., Odegova, T.F., (2014) Vopr. Biol. Med. Farm. Khim., 12 (2), p. 37; Zykova, S.S., Odegova, T.F., Boichuk, S.V., Galembikova, A.R., (2014) Pharm. Chem. J., 48 (11), p. 708; Mukovoz, P.P., Dvorskaya, O.N., Koz'Minykh, V.O., (2011) Izv. Vyssh. Uchebn. Zaved., Ser. Khim. Khim. Tekhnol., 54 (5), p. 96; Sheldrick, G.M., (2008) Acta Crystallogr., Sect. A, 64, p. 112
Correspondence Address Mukovoz, P.P.; Institute for Cellular and Intracellular Symbiosis, Ural Branch, Russian Academy of Sciences, ul. Pionerskaya 11, Russian Federation
Publisher Maik Nauka Publishing / Springer SBM
CODEN RJOCE
Language of Original Document English
Abbreviated Source Title Russ. J. Org. Chem.
Source Scopus