Reactions of N,N-(dialkyl)arylthioacetamides with dialkyl acetylenedicarboxylates / Kosterina M.F., Morzherin Yu.Yu., Tkachev A.V., Rybalova T.V., Gatilov Yu.V., Bakulev V.A. // Russian Chemical Bulletin. - 2002. - V. 51, l. 4. - P. 613-618.

ISSN:
10665285
Type:
Article
Abstract:
2-(Alkoxycarbonylmethylidene)-4-aryl-5-(dialkylamino)thiophen-3(2H)-ones were synthesized by condensation of N,N-(dialkyl)arylthioacetamides with dialkyl acetylene-dicarboxylates. Intermediate substituted vinylic sulfides were isolated. When heated or in the presence of an acid or a base, they undergo cyclization into thiophenes.
Author keywords:
Condensation; Dialkyl acetylenedicarboxylates; N,N-(dialkyl)arylthioacetamides; Thiophene
Index keywords:
alkyl group; carboxylic acid derivative; thioacetamide derivative; thiophene derivative; vinyl derivative; article; carbon nuclear magnetic resonance; chemical reaction; crystal structure; cyclization
DOI:
нет данных
Смотреть в Scopus:
https://www.scopus.com/inward/record.uri?eid=2-s2.0-0141609831&partnerID=40&md5=4b4f18807e03d36108820391afc73d01
Соавторы в МНС:
Другие поля
Поле Значение
Link https://www.scopus.com/inward/record.uri?eid=2-s2.0-0141609831&partnerID=40&md5=4b4f18807e03d36108820391afc73d01
Affiliations Ural State Technical University, 19 ul. Mira, 620002 Yekaterinburg, Russian Federation; N. N. Vorozhtsov Novosibirsk I., Siberian Br. Russ. Acad. of Sci., 9 prosp. Akad. Lavrent'eva, 630090 Novosibirsk, Russian Federation
Author Keywords Condensation; Dialkyl acetylenedicarboxylates; N,N-(dialkyl)arylthioacetamides; Thiophene
Chemicals/CAS vinyl derivative, 2669-89-8
References Hendrickson, H., Reeds, P., Templeton, J.F., (1964) J. Am. Chem. Soc., 86, p. 107; Berseneva, V.S., Morzherin, Yu.Yu., Dehaen, W., Luyten, I., Bakulev, V.A., (2001) Tetrahedron, 57, p. 2179; Berseneva, V.S., Tkachev, A.V., Morzherin, Yu.Yu., Dehaen, W., Luyten, I., Toppet, S., Bakulev, V.A., (1998) J. Chem. Soc., Perkin Trans. 1, p. 2133; Giannola, L.I., Giammona, G., Palazzo, S., Lamatrina, L., (1984) J. Chem. Soc., Perkin Trans. 1, p. 2707; Giannola, L.I., Palazzo, S., Agozzino, P., Lamatrina, L., Caraulo, L., (1978) J. Chem. Soc., Perkin Trans. 1, p. 1428; Coen, R., Ragonnet, B., Vieillescazes, C., Roggero, J.P., (1985) Heterocycles, 23 (5), p. 1225; Giammona, H., Neri, M., Carlisi, B., Pazzo, A., La Rosa, C., (1991) J. Heterocycl. Chem., 28, p. 325; Kurasawa, Yo., Ritsuko Katoh, R., Takada, A., Kim, H.S., Okamoto, Yo., (1992) J. Heterocycl. Chem., 29, p. 1001; Landreau, C., Deniaud, D., Reliquet, A., Reliquet, F., Meslin, J.C., (2001) J. Heterocycl. Chem., 38, p. 93; Chumakov, Yu.M., Akkurt, M., Enal, A., Mazus, M.D., Dimoglo, A.S., Malinovskii, T.I., (1996) Kristallografiya, 41, p. 869; (1996) Crystallogr. Repts., 41. , Engl. Transl; L'abbe, G., Huybrechts, L., Toppet, S., Declerq, J.P., Germain, G., Van Meerssche, M., (1978) Bull. Soc. Chim. Belg., 87, p. 893
Correspondence Address Morzherin, Yu.Yu.; Ural State Technical University, 19 ul. Mira, 620002 Yekaterinburg, Russian Federation; email: morjerine@htf.ustu.ru
Language of Original Document English
Abbreviated Source Title Russ. Chem. Bull.
Source Scopus