Two directions of cyclization of α-diazo-β-dithioamides. New rearrangements of 12,3,-triazole-4-carbothiamides. / Bakulev V.A., Lebedev A.T., Dankova E.F., Mokrushin V.S., Petrosyan V.S. // Tetrahedron. - 1989. - V. 45, l. 23. - P. 7329-7340.

ISSN:

00404020

Type:

Article

Abstract:

The cyclization processes of 2-diazomalondithioamides, generated by five different methods, have been studied. The ambient character of the derivatives of 2-diazomalondithioamide is the cause of previously unknown rearrangements of 5-mereapto-1,2,3-triazole- and 5-amino-1,2,3-thiadiazole-4-N-R-carbothioamides to 5-N-R-amino-1,2,3-thiadiazole-4-carbothioamides. NMR 1H and 13C spectra and mass-spectra are presented for the series of 5-amino-1,2,3-thiadiazole derivatives. © 1989.

Author keywords:

Index keywords:

нет данных

DOI:

10.1016/S0040-4020(01)89194-8

Смотреть в Scopus:

https://www.scopus.com/inward/record.uri?eid=2-s2.0-25444476925&doi=10.1016%2fS0040-4020%2801%2989194-8&partnerID=40&md5=b03615be2f14dfeb09e8a83251ef8b77

Соавторы в МНС:

—

Другие поля

Поле	Значение
Link	https://www.scopus.com/inward/record.uri?eid=2-s2.0-25444476925&doi=10.1016%2fS0040-4020%2801%2989194-8&partnerID=40&md5=b03615be2f14dfeb09e8a83251ef8b77
Affiliations	Department of Technology of_Organic Compounds, Polytechnic Institute Sverdlovsk, Russian Federation; Department of Chemistry, M.V. Lomonosov University, Moscow, 119899, Russian Federation
References	L'Abbē, (1984) J. Heterocycl. Chem., 21, p. 627; Bakulev, Mokrushin, (1986) Khim. Geterotsikl. Soed., p. 1421; Regitz, Sherer, Umlagerungsreaktionen, IV. Über die Dimroth-Umlagerung im System 5-Amino-1.2.3-thiadiazol/5-Mercapto-1.2.3-triazol (1969) Chemische Berichte, 102, p. 417; Bakulev, Shafran, Mokrushin, Pushkareva, (1982) Khim. Geterotsikl. Soed., p. 1696; Kolobov, Bakulev, Mokrushin, (1987) Z. Org. Khim., 23, p. 1120; Konstantinova, (1982) Byulletem' Izobreteniy., 33, p. 133. , Pat. 2990162 (USSR); Nakai, Harada, Mori, (1984) C.A., 100, p. 72730. , Pat. 31548 (Eur); Kumkazu, (1984) C.A., 100, p. 72730. , Pat. 1O3840 (Eur); Shafran, Bakulev, Mokrushin, Kondratiev, (1983) Byulleten' Izobreteniy., 43, p. 79. , Pat. 1055741 (USSR); Lebedev, Shevchenko, Kazaryan, Bakulev, Shafran, Kolobov, Petrosyan, (1987) Khim. Geterotsikl. Soed., p. 681; Lebedev, Samguina, Sharbatyan, Bakulev, Dankova, Petrosyan, (1988) Khim. Geterotsikl. Soed., p. 118; Grabenko, Pelkis, Kulaeva, (1962) Z. Ob. Khim., 32, p. 2240; Levi, Nelson, (1972) Carbon-13 Nuclear Magnetic Resonance for Organic Chemists, , Wiley-Interscience; Shafran, Bakulev, Mokrushin, Alekseev, (1984) Khim. Geterotsikl. Soed., p. 1266; Shafran, Bakulev, Mokrushin, Validuda, (1986) Khim. Geterotsikl. Soed., p. 691; Dankova, Bakulev, Mokrushin, Sidorov, Lebedev, (1987) Khim. Geterotsikl. Soed., p. 845; Cava, Levinson, (1985) Tetrah. Lett., 41, p. 5061; Bakulev, Mokrushin, Grishakov, Pushkareva, (1982) Khim. Geterotsikl. Soed., p. 957
Correspondence Address	Bakulev, V.A.; Department of Technology of_Organic Compounds, Polytechnic Institute SverdlovskRussian Federation
CODEN	TETRA
Language of Original Document	English
Abbreviated Source Title	Tetrahedron
Source	Scopus