Small-angle neutron scattering from samples of expanded carbon / Bogdanov S.G., Valiev É.Z., Dorofeev Yu.A., Pirogov A.N., Skryabin Yu.N., Makotchenko V.G., Nazarov A.S., Fedorov V.E. // Crystallography Reports. - 2006. - V. 51, l. SUPPL. 1. - P. S12-S15.

ISSN:
10637745
Type:
Conference Paper
Abstract:
The subatomic structure of expanded graphite has been investigated by small-angle neutron scattering. Samples were synthesized during quick thermal decomposition of intercalated compounds based on oxidized graphite. They had a low bulk density (up to 0.1 g/cm3) and were characterized by considerable small-angle scattering. It has been established that majority of the volume of expanded graphite samples is occupied by participles with characteristic sizes in two ranges: from 6 to 8 nm and from 20 to 30 nm. Small particles have properties of a surface fractal with the dimension D s = 2.4-2.6, whereas the larger particles are mainly smooth and have the dimension D s = 2.0-2.1. The specific surface of the samples studied was determined from the small-angle scattering data. © Nauka/Interperiodica 2006.
Author keywords:
Index keywords:
Data reduction; Fractals; Graphite; Intercalation compounds; Molecular structure; Pyrolysis; Bulk density; graphite; Small angle scattering; Subatomic structure; Neutron scattering
DOI:
10.1134/S1063774506070030
Смотреть в Scopus:
https://www.scopus.com/inward/record.uri?eid=2-s2.0-33751557475&doi=10.1134%2fS1063774506070030&partnerID=40&md5=b52db483b7cc9da73b2c18216bb5d167
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Affiliations Institute of Metal Physics, Ural Division, Russian Academy of Sciences, ul. Sof'i Kovalevskoǐ 18, Yekaterinburg, 620041, Russian Federation; Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent'eva 3, Novosibirsk, 630090, Russian Federation
References Mahajan, V.K., (1974) Inorg. Nucl. Chem. Lett., 10, p. 1103; Nazarov, A.S., Makotchenko, V.G., (2002) Neorg. Mater., 38 (3), p. 351; Lukashin, A.V., Kalinin, S.V., Vergel, A.A., Tret'yakov, Yu.D., (1999) Dokl. Akad. Nauk, 369 (6), p. 781; Schaefer, D.W., Keefer, K.D., (1986) Fractals in Physics, , Ed. by L. Pietronero and E. Tosatti (North-Holland, Amsterdam; Mir, Moscow); Bale, H.D., Schmidt, P.W., (1984) Phys. Rev. Lett., 53, p. 596; Debye, P., Anderson, H.R., Brumberger, H., (1957) J. Appl. Phys., 28, p. 679; Valiev, É.Z., Ostroushko, A.A., Bogdanov, S.G., (2001) Poverkhnost, 11, p. 38; Teplykh, A.E., Bogdanov, S.G., Dorofeev, Yu.A., (2006) Crystallography Reports, 51 (SUPPL.), pp. S62; Valiev, É.Z., Bogdanov, S.G., Pirogov, A.N., Kuklin, A.I., (2002) Poverkhnost, 9, p. 59; Svergun, D.I., Feǐgin, L.A., (1986) X-ray and Neutron Small-angle Scattering, , (Nauka, Moscow) [in Russian]
Correspondence Address Bogdanov, S.G.; Institute of Metal Physics, Ural Division, Russian Academy of Sciences, ul. Sof'i Kovalevskoǐ 18, Yekaterinburg, 620041, Russian Federation; email: sbogdanov@uraltc.ru
Language of Original Document English
Abbreviated Source Title Crystallogr. Rep.
Source Scopus