Synthesis of analogs of 5(4)-aminoimidazole-4(5)-carboxamide and purines - V. Some transformations in the imidazo[4,5-d]-1,2,3-triazine series / Mokrushin V.S., Ofitserov V.I., Rapakova T.V., Tsaur A.G., Pushkareva Z.V. // Chemistry of Heterocyclic Compounds. - 1977. - V. 12, l. 4. - P. 465-468.

ISSN:
00093122
Type:
Article
Abstract:
4-Chloroimidazo[4,5-d]-1,2,3-triazine was obtained by oxidative chlorinatlon from imidazo[4,5-d]-1,2,3-triazine-4-thione, and its reaction with nucleophilic agents and cleavage of the triazine ring to give 5-diazoimidazole-4-carbonitrile were studied. The newly synthesized diazoimidazole was subjected to C- and N-diazo coupling. It was established that 3-methylimidazo[4,5-d]-1,2,3-triazine-4-imine, formed by reaction of the diazo compound with methylamine, is capable of recyclization to 4-methylaminoimidazo[4,5-d]-1,2,3-triazine. © 1977 Plenum Publishing Corporation.
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DOI:
10.1007/BF00480442
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Affiliations S. M. Kirov Ural Polytechnic Institute, Sverdlovsk, Russian Federation
References Ofitserov, V.I., Mokrushin, V.S., Pushkareva, Z.V., Nifontov, V.I., Nikiforova, N.V., Lych, L.N., (1975) Khim. Geterotsikl. Soedin., 11, p. 1550; Stanovnik, B., Tisler, M., PYRIDO(3,2-d)-v-TRIAZIN-4(3H)-ONE (1972) Organic Preparations and Procedures International, 4 (2), p. 55; Shealy, Y.F., Struck, R.F., Holum, L.B., Montgomery, J.A., (1961) J. Org. Chem., 26, p. 2396; Stevens, H.N.E., Stevens, M.F.G., (1970) J. Chem. Soc., C, 6, p. 765; Pushkareva, Z.V., Ofitserov, V.I., Mokrushin, V.S., Aglitskaya, K.V., (1975) Khim. Geterotsikl. Soedin., 8, p. 1141; Yamazaki, S., Meguro, T., Kumashiro, I., (1969) Chem. Abstr., 70. , 78,011
Correspondence Address Mokrushin, V.S.; S. M. Kirov Ural Polytechnic Institute, Sverdlovsk, Russian Federation
Publisher Kluwer Academic Publishers-Plenum Publishers
CODEN CHCCA
Language of Original Document English
Abbreviated Source Title Chem Heterocycl Compd
Source Scopus