Formation of macro- and microstructure during the beta ->alpha transformation in zirconium single crystals / Khlebnikova Yu. V.,Sazonova V. A.,Rodionov D. P.,Vil'danova N. F.,Egorova L. Yu.,Kaletina Yu. V.,Solodova I. L.,Umova V. M. // PHYSICS OF METALS AND METALLOGRAPHY. - 2009. - V. 108, l. 3. - P. 254-262.

ISSN/EISSN:

0031-918X / нет данных

Type:

Article

Abstract:

Structure of an iodide zirconium single crystal prepared by zone melting has been studied by X-ray diffraction and optical and electron microscopy. It has been shown that the initial single crystal consists of macroscopic hcp packets, which are revealed by etching in crystal sections and differ in shape and dimensions (0.3-0.8 cm(2)). The orientation of each packet obeys the Burgers orientational relationships. Five different orientations of hcp packets of six possible variants have been found. The microstructure of each of such regions consists of a set of laths of the alpha phase of identical orientation separated by low-angle dislocation boundaries. The existence of structural heredity in the zirconium single crystal after a cycle of alpha ->beta -> I +/- transformations at the rate of heating and cooling on the order of 4-5 K/s has been confirmed. After quenching of a pseudo-single crystal of zirconium from a temperature of 960A degrees C in a 10\% NaCl solution, the packet structure of the alpha phase is retained, but the dimensions of the laths decrease severalfold.

Author keywords:

нет данных

DOI:

10.1134/S0031918X09090063

Web of Science ID:

ISI:000270327800006

Соавторы в МНС:

—

Другие поля

Поле	Значение
Month	SEP
Publisher	MAIK NAUKA/INTERPERIODICA/SPRINGER
Address	233 SPRING ST, NEW YORK, NY 10013-1578 USA
Language	English
Research-Areas	Metallurgy \& Metallurgical Engineering
Web-of-Science-Categories	Metallurgy \& Metallurgical Engineering
ResearcherID-Numbers	Kaletina, Julia/K-6257-2013 Solodova, Irina/K-3740-2013 Egorova, Lada/J-3564-2013 Khlebnikova, Yulia/K-2076-2013 Rodionov, Dmitry/K-3552-2013
ORCID-Numbers	Kaletina, Julia/0000-0001-7452-6951 Solodova, Irina/0000-0002-0835-2946 Egorova, Lada/0000-0002-1951-2976 Khlebnikova, Yulia/0000-0003-2196-1647 Rodionov, Dmitry/0000-0002-8366-0279
Funding-Acknowledgement	Russian Academy of Sciences {[}01.2.006 13392]; {[}NSh-643.2008.3]
Funding-Text	The electron-microscopic studies were performed in the Center of Electron Microscopy of Collective Use, Institute of Metal Physics, Ural Division, Russian Academy of Sciences. This work was performed according to the plan of the Russian Academy of Sciences ( theme no. 01.2.006 13392) and was supported in part by the grant NSh-643.2008.3.
Number-of-Cited-References	11
Usage-Count-Since-2013	4
Journal-ISO	Phys. Metals Metallogr.
Doc-Delivery-Number	500TL