Determination of enantiomeric purity of 1-substituted 3-amino-1,2-dicarba-closo-dodecaboranes by HPLC on chiral stationary phases / Krasnov V. P.,Demin A. M.,Levit G. L.,Grishakov A. N.,Sadretdinova L. Sh.,Ol'shevskaya V. A.,Glukhov I. V.,Kalinin V. N.,Charushin V. N. // RUSSIAN CHEMICAL BULLETIN. - 2008. - V. 57, l. 12. - P. 2535-2539.

ISSN/EISSN:
1066-5285 / нет данных
Type:
Article
Abstract:
A determination of enantiomeric purity of 1-substituted (Me, Ph, and Pr(i)) 3-amino-1,2dicarba-closo-dodecaboranes by HPLC on chiral Chiralcel OD-H and Chiralpac AD stationary phases involving preliminary phthaloylation of 3-aminocarboranes has been suggested as a general method.
Author keywords:
carboranes; enantiomers; HPLC; chiral stationary phases; kinetic resolution PRESSURE LIQUID-CHROMATOGRAPHY; DICARBA-CLOSO-DODECABORANES; NEUTRON-CAPTURE THERAPY; ASYMMETRIC COBALTACARBORANES; RESOLUTION; DERIVATIVES; CHEMISTRY; DERIVATIZATION; CARBORANES; SEPARATION
DOI:
10.1007/s11172-008-0364-5
Web of Science ID:
ISI:000207482900014
Соавторы в МНС:
Другие поля
Поле Значение
Month DEC
Publisher SPRINGER
Address 233 SPRING ST, NEW YORK, NY 10013 USA
Language English
Keywords-Plus PRESSURE LIQUID-CHROMATOGRAPHY; DICARBA-CLOSO-DODECABORANES; NEUTRON-CAPTURE THERAPY; ASYMMETRIC COBALTACARBORANES; RESOLUTION; DERIVATIVES; CHEMISTRY; DERIVATIZATION; CARBORANES; SEPARATION
Research-Areas Chemistry
Web-of-Science-Categories Chemistry, Multidisciplinary
Author-Email ca@ios.uran.ru
ResearcherID-Numbers Demin, Alexander/L-7353-2016
ORCID-Numbers Demin, Alexander/0000-0002-4132-2327
Funding-Acknowledgement Russian Foundation for Basic Research {[}07-03-00684]; International Scientific and Technical Center {[}3477]; Russian Federation President Council {[}NSh 3758.2008.3]
Funding-Text This work was financially supported by the Russian Foundation for Basic Research (Project No. 07-03-00684), the International Scientific and Technical Center (Grant 3477), and the Russian Federation President Council for Grants (Program for the State Support of Leading Scientific Schools, Grant NSh 3758.2008.3).
Number-of-Cited-References 33
Usage-Count-Since-2013 1
Journal-ISO Russ. Chem. Bull.
Doc-Delivery-Number V10SE