Reaction of 3,4-dioxohexane-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine / Mukovoz P.P., Koz’minykh V.O., Slepukhin P.A., Ganebnykh I.N., El’tsov O.S., Gorbunova A.V., Koz’minykh E.N. // Russian Journal of Organic Chemistry. - 2016. - V. 52, l. 5. - P. 636-643.

ISSN:
10704280
Type:
Article
Abstract:
Reaction was studied of 3,4-dihydroxyhexa-2,4-diene-1,6-dioic acid esters with 2,4-dinitrophenylhydrazine that led to the formation of esters of (3E)-3-[2-(2,4-dinitrophenyl)-hydrazinylidene]-4-oxohexane-1,6-dioic and (3E,4E)-3,4-bis[2-(2,4-dinitrophenyl)hydrazinylidene]-hexane-1,6-dioic acids. The structural features of compounds synthesized were established from the data of IR and NMR spectra and X-ray diffraction (XRD) analysis. © 2016, Pleiades Publishing, Ltd.
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DOI:
10.1134/S1070428016050043
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Affiliations Moscow Technologic Institute, Orenburg Branch, pr. Pobedy 75, Orenburg, Russian Federation; Perm State Humanitarian and Pedagogical University, Perm, Russian Federation; Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, Yekaterinburg, Russian Federation; El’tsin Ural Federal University, Yekaterinburg, Russian Federation; Orenburg State University, Orenburg, Russian Federation
References Fusko, R., Zumin, S., (1946) Gazz. Chim. Ital., 76, p. 223; Finar, I.L., (1955) J. Chem. Soc., p. 1205; Shironina, T.M., Igidov, N.M., Koz’minykh, E.N., Kon’shina, L.O., Kasatkina, Y.S., Koz’minykh, V.O., (2001) Russ. J. Org. Chem., 37, p. 1486. , COI: 1:CAS:528:DC%2BD38XhtlKls74%3D; Perevalov, S.G., Burgart, Y.V., Saloutin, V.I., Chupakhin, O.N., (2001) Russ. Chem. Rev., 70, p. 921. , COI: 1:CAS:528:DC%2BD38XjtVOisr0%3D; Mukovoz, P.P., Koz’minukh, V.O., (2009) Vestn. Yuzhno-Ural. Gos. Univer., p. 4; Bellami, L., (1963) Infrakrasnye spektry slozhnykh molekul, , Inostrannaya Literatura, Moscow; International Tables for Crystallography, 2006, vol. C, p. 790; Andreeva, V.A., Mukovoz, P.P., Slepukhin, P.A., El’tsov, O.S., Koz’minykh, E.N., Koz’minykh, V.O., (2015) Innovatsionnye tekhnologii v nauke i obrazovanii. Materialy II mezhdynarodnoi nauchno-prakticheskoi konferentsii, p. 20; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J., Howard, J.A.K., Puschmann, H., (2009) J. Appl. Cryst., 42, p. 339. , COI: 1:CAS:528:DC%2BD1MXjsFSnsbg%3D; Koz’minykh, V.O., Mukovoz, P.P., Kirillova, E.A., (2009) Vestn. Orenburg. Gos. Univer., p. 155; Mukovoz, P.P., Dvorskaya, O.N., Koz’minykh, V.O., (2011) Izv. Vuzov, Ser. Khim. Khim. Tekhnol., 54, p. 96. , COI: 1:CAS:528:DC%2BC3MXovF2rtbs%3D
Correspondence Address Mukovoz, P.P.; Moscow Technologic Institute, Orenburg Branch, pr. Pobedy 75, Russian Federation; email: mpp27@mail.ru
Publisher Maik Nauka Publishing / Springer SBM
CODEN RJOCE
Language of Original Document English
Abbreviated Source Title Russ. J. Org. Chem.
Source Scopus